Reaktion #412765

Reaktionsgleichung

p-Dioxanone

2,5-morpholinedione

stannous octoate

→

p-Dioxanone 2,5-Morpholinedione

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONmagnetically mixed in
2. 2
   Temperatura flame
3. 3
   Sonstigevacuum dried
4. 4
   Sonstigesealed glass ampoule

Vorschrift

p-Dioxanone (4.0 g, 0.039 moles), 2,5-morpholinedione (0.5 g, 0.0043 moles) and a catalytic amount of stannous octoate (0.22 ml of a 0.0132 M toluene solution, 0.0000029 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:

Quelle