Reaktion #412764

Reaktionsgleichung

p-Dioxanone

2.5-morpholinedione

1-dodecanol

stannous octoate

→

p-Dioxanone 2,5-Morpholinedione

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONmagnetically mixed in
2. 2
   Temperatura flame
3. 3
   Sonstigevacuum dried
4. 4
   Sonstigesealed glass ampoule

Vorschrift

p-Dioxanone (17.7 g, 0.174 moles), 2.5-morpholinedione (1.0 g, 0.00870 moles), 1-dodecanol (0.558 g, 0.000299 moles), and a catalytic amount of stannous octoate (0.46 ml of a 0.0264 M toluene solution, 0.000021 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:

Quelle