Reaktion #412761

Reaktionsgleichung

p-Dioxanone

2,5-morpholinedione

1-dodecanol

stannous octoate

→

p-Dioxanone 2,5-Morpholinedione

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONmagnetically mixed in
2. 2
   Temperatura flame
3. 3
   Sonstigevacuum dried
4. 4
   Sonstigesealed glass ampoule

Vorschrift

p-Dioxanone (87.8 g, 0.861 moles), 2,5-morpholinedione (1.0 g, 0.0087 moles), 1-dodecanol (0.27 g, 0.00145 moles) and a catalytic amount of stannous octoate (0.176 ml of 0.33 M toluene solution, 0.000058 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:

Quelle