Reaktion #412096

Reaktionsgleichung

Phenoxyacetic acid

thionyl chloride

→

phenoxyacetyl chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeAfter the 5 end of the reaction
2. 2
   Einengenthe reaction mixture was concentrated under vacuum at 300 C

Vorschrift

Phenoxyacetic acid (d5) was treated with 25 ml of thionyl chloride and stirred for 18 hours at room temperature. After the 5 end of the reaction, the reaction mixture was concentrated under vacuum at 300 C to provide phenoxyacetyl chloride (4.8 g).

Quelle