Reaktion #40287

ord-128be03e30fc479198b6496eaff8785b

Reaktionsgleichung

CCOC(=O)CON
2-Aminoxy-acetic acid ethyl ester
C#CCCC(=O)O
4-Pentynoic acid
C(=NC1CCCCC1)=NC1CCCCC1
dicyclohexylcarbodiimide
C#CCCC(=O)NOCC(=O)OCC
Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07727713B2uspto-grants-2010_06