Reaktion #3847

ord-6da5e6fc912a4f39abb42807db3359a7

Reaktionsgleichung

CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1ccccn1
N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide
CC(=O)OO
peracetic acid
→
CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1cccc[n+]1[O-]
title compound
CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1cccc[n+]1[O-]
N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide 1-oxide

Edukte

CN(c1ncc(Cl)cc1Cl)S(=O)(=O)c1ccccn1
N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide
CC(=O)OO
peracetic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Following the procedures of Example 1, N-methyl-N-(3,5-dichloro-2-pyridyl)-2-pyridinesulfonamide is oxidized with 40% peracetic acid to give the title compound, MS m/e 334.00 (M+).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04722749uspto-grants-1988_02