Reaktion #3833
ord-ce2fac42f05a4292a71802d2a5aa59d9
Reaktionsgleichung
2,2'-dithiobisbenzoyl chloride
pyrrolidine
triethylamine
→
title compound
Ausbeute 60.6%
{2-[2-(pyrrolidine-1-carbonyl)-phenydisulfanyl]-phenyl}-pyrrolidin-1-yl-methanone
Ausbeute 60.6%
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1SonstigeThis compound was prepared
Vorschrift
This compound was prepared according to the general method of Example 112 using 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 15 mL of dichloromethane and pyrrolidine (0.63 mL, 7.5 mmol) and triethylamine (1.2 mL, 9 mmol) in 20 mL of dichloromethane, to give 0.75 g of the title compound as a foam, mp 62°-63° C.;