Reaktion #3832

Reaktionsgleichung

2,2'-dithiobisbenzoyl chloride

cyclopropylamine

triethylamine

dichloromethane

dichloromethane

→

title compound

2,2'-Dithiobis(N-cyclopropylbenzamide)

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeA solid formed immediately
2. 2
   Filtrationfiltered
3. 3
   SonstigeThe solid was dried

Vorschrift

A solution of 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 20 mL of dichloromethane was added dropwise to a solution of cyclopropylamine (0.52 mL, 7.5 mmol) and triethylamine (1.2 mL, 9.0 mmol) in 20 mL of dichloromethane. A solid formed immediately, the mixture was stirred for 3 hours and then filtered. The solid was dried to yield 0.65 g of the title compound, mp 257°-259° C.;

Quelle