Reaktion #3814

Reaktionsgleichung

2,2'-dithiobisbenzoyl chloride

3,5-dichloroaniline

→

title compound

Ausbeute 22.5%

2,2'-Dithiobis[N-(3,5-dichlorophenyl)benzamide]

Ausbeute 22.5%

Lösungsmittel

pyridine

dichloromethane

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis compound was prepared
2. 2
   SonstigeThe crude product was recrystallized from ethanol

Vorschrift

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 3,5-dichloroaniline (1.87 g, 11.7 mmol) in 15 mL of pyridine. The crude product was recrystallized from ethanol, then ethyl ether to yield 0.78 g of the title compound, mp 235°-236° C.

Quelle