Reaktion #3809

Reaktionsgleichung

2,2'-dithiobisbenzoyl chloride

3-bromoaniline

→

title compound

Ausbeute 55.8%

2,2'-Dithiobis[N-(3-bromophenyl)benzamide]

Ausbeute 55.8%

Lösungsmittel

pyridine

dichloromethane

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis compound was prepared
2. 2
   SonstigeThe crude product was recrystallized from ethyl acetate-hexanes

Vorschrift

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 3-bromoaniline (1.98 g, 11.6 mmol) in 16 mL of pyridine. The crude product was recrystallized from ethyl acetate-hexanes to yield 1.99 g of the title compound, mp 194°-196° C.

Quelle