Reaktion #3738
ord-712a4c23c26a4619a1659f080875532d
Reaktionsgleichung
1,3-di-cyclohexylmethyl-8-nitro xanthine
hydrobromic acid
→
title product
1,3-Di-cyclohexylmethyl-8-bromo Xanthine
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
The title compound was prepared from 1,3-di-cyclohexylmethyl-8-nitro xanthine (1 g, 0.0026 mol) and concentrated hydrobromic acid (40 ml, 48%) over 32 hours using an analogous procedure to that described in Example 15. The title product was obtained as a crystalline solid, m.pt. 247° C.