Reaktion #366152

Reaktionsgleichung

2-benzyloxy-6-chloro-5-cyano-benzo[de]isoquinoline-1,3-dione

2-Benzyloxy-6-chloro-5-cyano-benzo[de]isoquinoline-1,3-dione

piperidine

triethyl amine

→

title compound

Ausbeute 75.1%

2-Benzyloxy-5-cyano-6-(piperidin-1-yl)-benzo[de]isoquinoline-1,3-dione

Ausbeute 75.1%

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigewere reacted at ambient temperature for 5 hours

Vorschrift

Following the procedure of Example B2, 2-benzyloxy-6-chloro-5-cyano-benzo[de]isoquinoline-1,3-dione (0.20 g, 0.55 mmol, from Example A2), piperidine (0.11 g, 1.1 mmol), and triethyl amine (0.11 g, 1.1 mmol) were reacted at ambient temperature for 5 hours to give 0.17 g of the title compound.

Quelle