Reaktion #364240

Reaktionsgleichung

4-bromo-pyridine-2,6-diamine

O-mesitylene-sulfonylhydroxylamine

furfural

→

title compound

7-Bromo-2-furan-2-yl-[1,2,4]triazolo[1,5-a]pyridin-5-ylamine

Reaktionsbedingungen

Vorschrift

The title compound, MS m/e (%): 281 (M++2, 100), was prepared in accordance with the (general method of example 63 from 4-bromo-pyridine-2,6-diamine, O-mesitylene-sulfonylhydroxylamine, and furfural. The purification was performed with reversed phase HPLC eluting with an acetonitrile/water gradient.

Quelle