Reaktion #363860

ord-bbaba7aa49114553bafc341c695991fe

Reaktionsgleichung

Cc1cc([N+](=O)[O-])ccc1N=C=S
2-Methyl-4-nitrophenyl isothiocyanate
CCC(CC)CN
2-ethyl-1-butylamine
CC(Cl)C(=O)O
α-chloropropionic acid
→
CCC(CC)CN1C(=O)C(C)SC1=Nc1ccc([N+](=O)[O-])cc1C
2-(2-methyl-4-nitrophenylimino)-3-(2-ethyl-1-butyl)-5-methyl-1,3-thiazolidin-4-one

Edukte

Cc1cc([N+](=O)[O-])ccc1N=C=S
2-Methyl-4-nitrophenyl isothiocyanate
CCC(CC)CN
2-ethyl-1-butylamine
CC(Cl)C(=O)O
α-chloropropionic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

2-Methyl-4-nitrophenyl isothiocyanate was reacted with 2-ethyl-1-butylamine followed by α-chloropropionic acid according to Method C8a to afford 2-(2-methyl-4-nitrophenylimino)-3-(2-ethyl-1-butyl)-5-methyl-1,3-thiazolidin-4-one.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06353006B1uspto-grants-2002_03