Reaktion #362166

Reaktionsgleichung

indene

sodium

→

Indene Sodium Salt

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigereaction
2. 2
   Temperaturat reflux for 4 hours
3. 3
   SonstigeThereafter, unreacted sodium was removed
4. 4
   Sonstigea 2 mols/l THF solution was prepared

Vorschrift

50 ml of purified tetrahydrofuran (THF) was charged into a three-necked 300 ml flask, then 20 g of indene and 4 g of metal sodium were added, and reaction was allowed to take place at reflux for 4 hours. Thereafter, unreacted sodium was removed and then a 2 mols/l THF solution was prepared using the reaction product.

Quelle