Reaktion #359159

Reaktionsgleichung

trimethylchlorosilane

2-bromoindene

magnesium

→

Bromomagnesium indene

2-trimethylsilylindene

Reaktionsbedingungen

Vorschrift

Bromomagnesium indene was prepared from 10.0 g (51.3 mmol) of 2-bromoindene and 5 g of magnesium in a nitrogen stream. The reaction product was reacted with 6.5 ml of trimethylchlorosilane to obtain 7.14 g (37.9 mmol) of 2-trimethylsilylindene as a colorless oily product.

Quelle