Reaktion #358507

ord-bdc9faa410f04d1db0c6ff652e6c7d41

Reaktionsgleichung

COC(=O)c1c(Cl)cc(N(S(C)(=O)=O)S(C)(=O)=O)cc1Cl
2,6-dichloro-4-[bis(methanesulfonyl)amino] benzoic acid methylester
[Na+].[OH-]
sodium hydroxide
→
COC(=O)c1c(Cl)cc(NS(C)(=O)=O)cc1Cl
title compound
COC(=O)c1c(Cl)cc(NS(C)(=O)=O)cc1Cl
2,6-dichloro-4-methanesulfonylamino Benzoic Acid Methylester

Edukte

—
aqueous solution
COC(=O)c1c(Cl)cc(N(S(C)(=O)=O)S(C)(=O)=O)cc1Cl
2,6-dichloro-4-[bis(methanesulfonyl)amino] benzoic acid methylester
[Na+].[OH-]
sodium hydroxide

Reagenzien

Keine

Lösungsmittel

CCO
ethanol

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeAfter the solvent was removed
  2. 2
    workup.ADDITIONthe obtained substance was treated by an ordinary method

Vorschrift

The mixture of 100 mg of 2,6-dichloro-4-[bis(methanesulfonyl)amino] benzoic acid methylester, 3 ml of an aqueous solution of 1N sodium hydroxide and 10 ml of ethanol was stirred. After the solvent was removed, the obtained substance was treated by an ordinary method using ethyl acetate as an extractant to obtain the title compound.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07452905B2uspto-grants-2008_11