Reaktion #355062

Reaktionsgleichung

adamantane carboxylic acid chloride

homoveratrylamine

triethylamine

→

title product

N-(3,4-Dimethoxyphenylethyl)-1-adamantanecarboxamide

Lösungsmittel

ethyl acetate ethyl ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeCrystallize the residue
2. 2
   Sonstigeobtained

Vorschrift

Subject 2.0 g. of adamantane carboxylic acid chloride 1.8 g. (10.0 mmoles) of homoveratrylamine and 5.0 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from an ethyl acetate-ethyl ether mixture to obtain the title product, m.p. 132°-133°C.

Quelle