Reaktion #354749

Reaktionsgleichung

ammonia

trimethylchlorosilane

6-bromohexan-1-ol

→

ammonia

6-bromohexyloxytrimethylsilane

Lösungsmittel

benzene

Reaktionsbedingungen

Vorschrift

13.8 G. of trimethylchlorosilane and 11.4 g. of 6-bromohexan-1-ol are mixed together in 100 ml. of dry benzene and are stirred in an ice-bath while anhydrous ammonia is passed therethrough until the odor of ammonia persists to obtain 6-bromohexyloxytrimethylsilane, which is worked up by filtration, followed by evaporation of the filtrate and distillation in vacuo.

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