Reaktion #352366

ord-fbb04630f653448c8d5a53857ce1386f

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigethat described in Preparation 40

Vorschrift

Following a procedure similar to that described in Preparation 40, but using 3.2 g of 2-propylimidazole-4,5-dicarbonitrile (prepared as described in Preparation 10) and 33 ml of a 2M solution of t-butylmagnesium chloride in diethyl ether, 2.35 g of the title compound were obtained as crystals, melting at 176°-178° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05646171uspto-grants-1997_07