Reaktion #350556

Reaktionsgleichung

phthalonitrile

gallium trimethoxide

→

gallium phthalocyanine

Lösungsmittel

ethylene glycol

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe resulting product was then filtered
2. 2
   WaschenThe product was washed with N,N-dimethylformamide
3. 3
   Trocknenwith methanol, and then dried

Vorschrift

31.8 parts of phthalonitrile, 10.1 parts of gallium trimethoxide, and 150 ml of ethylene glycol were stirred at a temperature of 200° C. in an atmosphere of nitrogen for 24 hours. The resulting product was then filtered. The product was washed with N,N-dimethylformamide and then with methanol, and then dried to obtain 25.1 parts of gallium phthalocyanine.

Quelle