Reaktion #350301

ord-6197c8223165426bbd0b61e9191a5d45

Reaktionsgleichung

O=[N+]([O-])c1cc(C(F)(F)F)c(Cl)c([N+](=O)[O-])c1Cl
2,4-dichloro-3,5-dinitrobenzotrifluoride
CNN
methylhydrazine
→
CNNc1c([N+](=O)[O-])cc(C(F)(F)F)c(Cl)c1[N+](=O)[O-]
N-(methylamino)-3-chloro-2,6-dinitro-4-trifluoromethylaniline

Edukte

O=[N+]([O-])c1cc(C(F)(F)F)c(Cl)c([N+](=O)[O-])c1Cl
2,4-dichloro-3,5-dinitrobenzotrifluoride
CNN
methylhydrazine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe product was obtained
  2. 2
    Sonstigeto melt at 136°-137° C.

Vorschrift

The product was obtained by reacting 2,4-dichloro-3,5-dinitrobenzotrifluoride with methylhydrazine and found to melt at 136°-137° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04156083uspto-grants-1979_05