Reaktion #350300

ord-2d47f7269e794370b1dedbb4c3682f4d

Reaktionsgleichung

O=[N+]([O-])c1cc(Cl)c(Cl)cc1Cl
1,2,4-trichloro-5-nitrobenzene
CN(C)N
1,1-dimethylhydrazine
→
CN(C)Nc1cc(Cl)c(Cl)cc1[N+](=O)[O-]
desired product
CN(C)Nc1cc(Cl)c(Cl)cc1[N+](=O)[O-]
1,1-dimethyl-2-(3,4-dichloro-6-nitrophenyl)hydrazine

Edukte

O=[N+]([O-])c1cc(Cl)c(Cl)cc1Cl
1,2,4-trichloro-5-nitrobenzene
CN(C)N
1,1-dimethylhydrazine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Reaction of 1,2,4-trichloro-5-nitrobenzene with 1,1-dimethylhydrazine as described in Example I gave the desired product, m.p. 138°-143° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04156083uspto-grants-1979_05