Reaktion #348649

ord-095036f637844430aed6ef6a7890c047

Reaktionsgleichung

C=CC(=O)NCc1c(C)c2ccc(O)cc2oc1=O
acrylamido methyl 7-hydroxy-4-methyl coumarin
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearyl methacrylate
CC(C)(C#N)N=NC(C)(C)C#N
azobis-isobutyronitrile
→
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC.C=CC(=O)NCc1c(C)c2ccc(O)cc2oc1=O
acrylamido methyl-7-hydroxy-4-methyl coumarin stearyl methacrylate

Edukte

C=CC(=O)NCc1c(C)c2ccc(O)cc2oc1=O
acrylamido methyl 7-hydroxy-4-methyl coumarin
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearyl methacrylate
CC(C)(C#N)N=NC(C)(C)C#N
azobis-isobutyronitrile

Reagenzien

Keine

Lösungsmittel

CN(C)C=O
dimethylformamide

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeInto a 50 ml flask provided with a condenser
  2. 2
    Sonstigea nitrogen led in tube

Vorschrift

Into a 50 ml flask provided with a condenser, a nitrogen led in tube and an agitator, there are introduced 1 g of acrylamido methyl 7-hydroxy-4-methyl coumarin, 2 g of stearyl methacrylate, 0.3 g of azobis-isobutyronitrile and 6 g of dimethylformamide.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04166109uspto-grants-1979_08