Reaktion #348648

ord-09bee24ab4af46978f257e7b13a3a782

Reaktionsgleichung

[N].[Pb]
nitrogen lead
C=CC(=O)NCc1c(OC)ccc(C(=O)c2ccccc2)c1O
acrylamido methyl-4-methoxy-2-hydroxy benzophenone
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearyl methacrylate
CC(C)(C#N)N=NC(C)(C)C#N
azobis-isobutyronitrile
→
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC.C=CC(=O)NCc1c(OC)ccc(C(=O)c2ccccc2)c1O
acrylamido methyl-4-methoxy-2-hydroxy benzophenone stearyl methacrylate

Edukte

[N].[Pb]
nitrogen lead
C=CC(=O)NCc1c(OC)ccc(C(=O)c2ccccc2)c1O
acrylamido methyl-4-methoxy-2-hydroxy benzophenone
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearyl methacrylate
CC(C)(C#N)N=NC(C)(C)C#N
azobis-isobutyronitrile

Reagenzien

Keine

Lösungsmittel

CC(C)=O
acetone

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeInto a 50 ml flask provided with a condenser

Vorschrift

Into a 50 ml flask provided with a condenser, a nitrogen lead in tube and an agitator, there are introduced 2.5 g of acrylamido methyl-4-methoxy-2-hydroxy benzophenone, 2.5 g of stearyl methacrylate and 0.2 g of azobis-isobutyronitrile in solution in 10 g of acetone.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04166109uspto-grants-1979_08