Reaktion #348647

ord-ad05431320e545f5b396ab21c0d42f84

Reaktionsgleichung

CC(C)(C#N)N=NC(C)(C)C#N
azobis-isobutyronitrile
[N].[Pb]
nitrogen lead
C=CC(=O)NCc1cc(O)ccc1C(=O)c1ccccc1
acrylamido methyl 4-hydroxy benzophenone
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearyl methacrylate
→
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC.C=CC(=O)NCc1cc(O)ccc1C(=O)c1ccccc1
acrylamido methyl-4-hydroxy benzophenone stearyl methacrylate

Edukte

CC(C)(C#N)N=NC(C)(C)C#N
azobis-isobutyronitrile
[N].[Pb]
nitrogen lead
C=CC(=O)NCc1cc(O)ccc1C(=O)c1ccccc1
acrylamido methyl 4-hydroxy benzophenone
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearyl methacrylate

Reagenzien

Keine

Lösungsmittel

CC(C)=O
acetone

Reaktionsbedingungen

Temperatur
80°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeInto a 50 ml flask provided with a condenser

Vorschrift

Into a 50 ml flask provided with a condenser, a nitrogen lead in tube and an agitator, there are intorduced 1 g of acrylamido methyl 4-hydroxy benzophenone, 1.5 g of stearyl methacrylate and 0.25 g of azobis-isobutyronitrile in solution in 5 ml of acetone. The resulting mixture is heated for 8 hours at 80° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04166109uspto-grants-1979_08