Reaktion #347495

ord-670604e08b564c5a845c35fd9862e2cf

Reaktionsgleichung

C=CCOC(=O)C=Cc1ccc(OCC=C)c([N+](=O)[O-])c1
Allyl 4-allyloxy-3-nitrocinnamate
C=CCOC(=O)Cc1ccc(OCC=C)c([N+](=O)[O-])c1
allyl 4-allyloxy-3-nitrophenylacetate
→
C=CCOC(=O)Cc1ccc(OCC=C)c(N)c1
allyl 4-allyloxy-3-aminophenylacetate

Edukte

C=CCOC(=O)C=Cc1ccc(OCC=C)c([N+](=O)[O-])c1
Allyl 4-allyloxy-3-nitrocinnamate
C=CCOC(=O)Cc1ccc(OCC=C)c([N+](=O)[O-])c1
allyl 4-allyloxy-3-nitrophenylacetate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Allyl 4-allyloxy-3-nitrocinnamate was reduced by the method described in example 1 using allyl 4-allyloxy-3-nitrophenylacetate in place of allyl 3-nitrocinnamate, to give allyl 4-allyloxy-3-aminophenylacetate.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05527791uspto-grants-1996_06