Reaktion #344646

ord-b725b36d5ca04774ad2798ca293e30fc

Reaktionsgleichung

CCc1ccncc1
4-ethylpyridine
BrCCc1ccc(Br)cc1
4-bromophenethyl bromide
CC(CCc1ccc(Br)cc1)c1ccncc1
desired compound
Ausbeute 40.7%
CC(CCc1ccc(Br)cc1)c1ccncc1
1-(4-bromophenyl)-3-(4-pyridyl)-butane
Ausbeute 40.7%

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe reaction product was purified

Vorschrift

1.0 g (9.35 mmol) of 4-ethylpyridine and 2.47 g (9.35 mmol) of 4-bromophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.10 g of the desired compound (yield: 40.7%).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05262420uspto-grants-1993_11