Reaktion #344136

Reaktionsgleichung

methyl iodide

3-(4-(3-pentynyloxy)-1,2,5-thiadiazol-3-yl) pyridine

→

3-(4-(3-pentynyloxy)-1,2,5-thiadiazol-3-yl)-1-methylpyridinium iodide

Lösungsmittel

acetone

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe title compound precipitated from the solution
2. 2
   Filtrationwas collected by filtration
3. 3
   Sonstigeto yield 0.68 g (59%)

Vorschrift

A mixture of methyl iodide (0.6 ml, 9 mmol) and 3-(4-(3-pentynyloxy)-1,2,5-thiadiazol-3-yl) pyridine (3 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.68 g (59%).

Quelle