Reaktion #343480

Reaktionsgleichung

tetraethylene pentaamine

KOH

ethylene carbonate

→

ethylene carbonate triethylene tetraamine

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigefitted with a stirrer

Vorschrift

Add 56.7 g of tetraethylene pentaamine (with an AV of approximately 1050 mg KOH/g) to a 250 ml flask fitted with a stirrer, condensor and nitrogen inlet. Add 26.4 g ethylene carbonate to the system. Heat the system at 160° C. for 3 hours under N2. Strip the system to yield an ethylene carbonate-triethylene tetraamine adduct having an AV of approximately 410 mg KOH/g.

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