Reaktion #341764

ord-815f5380c7bf4c609ee37215b67dcb35

Reaktionsgleichung

CCc1ccc(OC)c(CC)c1CC1=NCCN1
2-(2,6-diethyl-3-methoxy-benzyl)-4,5-dihydro-1H-imidazole
CCc1ccc(OC)c(CC)c1CC1=NCCN1
2-(2,6-Diethyl-3-methoxy-benzyl)-4,5-dihydro-1H-imidazole
O=c1n(Cl)c(=O)n(Cl)c(=O)n1Cl
TCCA
C1CCC2=NCCCN2CC1
DBU
CCc1ccc(OC)c(CC)c1Cc1ncc[nH]1
2-(2,6-Diethyl-3-methoxy-benzyl)-1H-imidazole

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

2-(2,6-Diethyl-3-methoxy-benzyl)-1H-imidazole was prepared from 2-(2,6-diethyl-3-methoxy-benzyl)-4,5-dihydro-1H-imidazole (Example 206), TCCA and DBU in analogy to Example 194e): light yellow crystals; MS (ISP): 245.4 ([M+H]+, 100%).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07875645B2uspto-grants-2011_01