Reaktion #336056

Reaktionsgleichung

title compound

2-(N-Benzyl-N-methylamino)-1-(N-piperidinyl)ethane

→

title compound

2-(N-Methylamino)-1-(N-piperidinyl)ethane

Lösungsmittel

EtOH

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigeat room temperature
2. 2
   Sonstigefor 17 hours
3. 3
   FiltrationThe mixture was filtered
4. 4
   Einengenconcentrated

Vorschrift

A solution of the title compound of Step 11 (1.85 g, 7.96mmol) and 20% Pd(OH)2 on carbon in EtOH (50 mL) was placed under a hydrogen atmosphere (60 psi) at room temperature for 17 hours. The mixture was filtered and concentrated to give the title compound as a clear, yellow liquid (1.02 g, 90% crude yield). The proton spectral data were consistent with the proposed structure.

Quelle