Reaktion #3360

Reaktionsgleichung

4-chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide

sodium hydrogen sulfide

→

title compound

Ausbeute 65.2%

4-Mercapto-2-phenyl-pyrimidine-5-carboxylic acid benzylamide

Ausbeute 65.2%

Reaktionsbedingungen

Vorschrift

Using the procedure from Preparation 34, 5.8 g (17.9 mmol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide was reacted with 5.1 g (72 mmol) of sodium hydrogen sulfide to give 3.75 g of the title compound, mp 189°-193° C.

Quelle