Reaktion #335347

Reaktionsgleichung

hexadecanol

dimethylaminopyridine

ethyl 2-bromomethyl-2-propenoate

→

desired product

Ethyl 2-[(hexadecyloxy]methyl]-2-propenoate

Lösungsmittel

methylene chloride

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe solvent is evaporated

Vorschrift

To a stirred solution of 1.9 g of hexadecanol in 40 ml of methylene chloride containing 700 mg of dimethylaminopyridine is added 500 mg of ethyl 2-bromomethyl-2-propenoate followed by continued stirring for 18 hours. The solvent is evaporated to give 2.4 g of the desired product.

Quelle