Reaktion #335114

Reaktionsgleichung

product

2-(Tetradecyloxy)benzenemethanol

acetonitrile

phosphorus tribromide

→

title compound

1-(Bromomethyl)-2-(tetradecyloxy)benzene

Lösungsmittel

pyridine

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe product, 2.58 g, is obtained as cream crystals

Vorschrift

The title compound is prepared by the procedure of Example 20 using 2.5 g of product from Example 21, 10 ml acetonitrile, 2.11 g of phosphorus tribromide and 0.339 g of pyridine. The reaction is cooled for 10 minutes at 0° C., followed by stirring at room temperature for 1 hour. The product, 2.58 g, is obtained as cream crystals.

Quelle