Reaktion #334786

ord-f714e5e752f6466a82b3a3721d90bafe

Reaktionsgleichung

C=CCC12C=CC(C1)C1C(=O)OC(=O)C12
allylbicylo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride
Nc1ccc(O)cc1
4-aminophenol
O
water
→
C=CCC12C=CC(C1)C(C(=O)O)C2C(O)=Nc1ccc(O)cc1
Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid N-(4'-hydroxyphenyl)imide

Edukte

C=CCC12C=CC(C1)C1C(=O)OC(=O)C12
allylbicylo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride
Nc1ccc(O)cc1
4-aminophenol
O
water

Reagenzien

Keine

Lösungsmittel

Cc1ccccc1
toluene

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeis separated in a Hahn stillhead

Vorschrift

A solution of 101 g of allylbicylo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride and 54.5 g of 4-aminophenol in 155 g of toluene is heated to boiling point, and the water formed during imidation is separated in a Hahn stillhead.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04709047uspto-grants-1987_11