Reaktion #328711

ord-f376af89d306464aa7bfeb7248ea883f

Reaktionsgleichung

O=P([O-])([O-])[O-].[Na+].[Na+].[Na+]
sodium phosphate
[Cl-].[Na+]
sodium chloride
OCc1ccccc1
benzyl alcohol
C[C@H](CCC(=O)O)[C@H]1CC[C@H]2[C@@H]3CC[C@@H]4C[C@H](O)CC[C@]4(C)[C@H]3C[C@H](O)[C@]12C
deoxycholic acid
→
C[C@H](CCC(=O)[O-])[C@H]1CC[C@H]2[C@]3(C)CC[C@@H]4C[C@H](O)CC[C@]4(C)[C@H]3C[C@H](O)[C@]12C.[Na+]
sodium deoxycholate

Edukte

O=P([O-])([O-])[O-].[Na+].[Na+].[Na+]
sodium phosphate
[Cl-].[Na+]
sodium chloride
OCc1ccccc1
benzyl alcohol
C[C@H](CCC(=O)O)[C@H]1CC[C@H]2[C@@H]3CC[C@@H]4C[C@H](O)CC[C@]4(C)[C@H]3C[C@H](O)[C@]12C
deoxycholic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A composition of sodium deoxycholate (0.5% and 1%) was prepared comprising sodium phosphate (10 mM), sodium chloride (75-90 mM), benzyl alcohol (0.9%), deoxycholic acid, pH 8.3.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08653058B2uspto-grants-2014_02