Reaktion #327728

Reaktionsgleichung

4-(benzyloxy)-2-chloropyridine

hydrazine

→

crude product

1-(4-(benzyloxy)pyridin-2-yl)hydrazine

Lösungsmittel

pyridine

Reaktionsbedingungen

Aufarbeitung

1. 1
   TemperaturAfter heating
2. 2
   Temperaturto reflux for 18 hours
3. 3
   Einengenthe mixture was concentrated

Vorschrift

To a solution of 4-(benzyloxy)-2-chloropyridine (4.89 g, 22.30 mmol) in pyridine (120 mL) was added hydrazine (45 mL, 22.30 mmol). After heating to reflux for 18 hours, the mixture was concentrated to provide the crude product, which was used without further purification.

Quelle