Reaktion #324942

Reaktionsgleichung

1-benzyloxy-4-(3,3-dimethyl-cyclohex-1-enyl)-benzene

→

title compound

Ausbeute 102.4%

4-(3,3-Dimethyl-cyclohexyl)-phenol

Ausbeute 102.4%

Lösungsmittel

MeOH

EtOAc

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe reaction mixture was filtered through celite
2. 2
   EinengenThe filtrate was concentrated

Vorschrift

To 1-benzyloxy-4-(3,3-dimethyl-cyclohex-1-enyl)-benzene (4.3 g, 16.4 mmol) in MeOH (50 mL) and EtOAc (50 mL) was added 10% Pd/C (0.67 g) under N2. This mixture was stirred under H2 (1 atm) overnight. The reaction mixture was filtered through celite. The filtrate was concentrated to give the title compound as a white solid (3.43 g).

Quelle