Reaktion #323669

ord-2c6657bae82a4b1296b2e1595727200f

Reaktionsgleichung

CCCCCCCCCCCCCCCC(=O)OC(CCCCCCCCCCCCCCC)CC(=O)O
3-hexadecanoyloxyoctadecanoic acid
NCC(=O)O
glycine
→
CCCCCCCCCCCCCCCC(=O)OC(CCCCCCCCCCCCCCC)CC(=O)NCC(=O)O
N-(3-hexadecanoyloxyoctadecanoyl)glycine
Ausbeute 58.8%

Edukte

CCCCCCCCCCCCCCCC(=O)OC(CCCCCCCCCCCCCCC)CC(=O)O
3-hexadecanoyloxyoctadecanoic acid
NCC(=O)O
glycine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeprepared by the method

Vorschrift

Starting from 3-hexadecanoyloxyoctadecanoic acid (400 mg) prepared by the method described in Preparation 2 and glycine (300 mg), N-(3-hexadecanoyloxyoctadecanoyl)glycine (260 mg) was obtained as powders according to a similar manner to that of Preparation B-1.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04643990uspto-grants-1987_02