Reaktion #323667

ord-458ed4758049440a8471931fa59a60e2

Reaktionsgleichung

CCCCCCCCCCCCCCCC(=O)OC(CCCCCCCCCCCCCCC)CC(=O)O
3-hexadecanoyloxyoctadecanoic acid
NCCC(=O)O
β-alanine
→
CCCCCCCCCCCCCCCC(=O)OC(CCCCCCCCCCCCCCC)CC(=O)NCCC(=O)O
N-[3-hexadecanoyloxyoctadecanoyl]-β-alanine
Ausbeute 76.3%

Edukte

CCCCCCCCCCCCCCCC(=O)OC(CCCCCCCCCCCCCCC)CC(=O)O
3-hexadecanoyloxyoctadecanoic acid
—
( 5 )
NCCC(=O)O
β-alanine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeprepared by the method

Vorschrift

Starting from 3-hexadecanoyloxyoctadecanoic acid (10.8 g) prepared by the method described in Preparation A-2 (5) and β-alanine (5.36 g), N-[3-hexadecanoyloxyoctadecanoyl]-β-alanine (9.33 g) was obtained as crystals according to a similar manner to that of Preparation B-1.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04643990uspto-grants-1987_02