Reaktion #319054

Reaktionsgleichung

DCTA bromide

DMF

triethylamine

acetic

→

DCTA

Lösungsmittel

oxygen

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeAfter reaction the mixture

Vorschrift

One millimole of DCTA-bromide was added to 5 ml of DMF containing 0.2 ml of 1,2-dithioethylene and 0.5 ml of triethylamine. The mixture was incubated under argon for 2 hours at 60°-70° C. After reaction the mixture was diluted with oxygen-free H2O to 50 ml, the pH was adjusted to 4.0-4.5 with glacial acetic

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