Reaktion #318548

ord-d21a3434e0434b2981ada411456b3204

Reaktionsgleichung

C=CC(=C)C
isoprene
Nc1ccccc1N
200g
Nc1ccccc1N
1,2-Phenylenediamine
Nc1cccc(N)c1
1,3-phenylenediamine
C=CC(=C)C.Nc1cccc(N)c1
1,3-Phenylenediamine Isoprene

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A 200g (1.85 mol) portion of 1,3-phenylenediamine was alkenylated with 189g (2.77 mol) of isoprene in the same manner as shown in example 10. Product analysis by gas chromatography on isoprene and pentane free sample afforded the following assay.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04845291uspto-grants-1989_07