Reaktion #317763

ord-97941ee5c09242bd8528532cf13dd359

Reaktionsgleichung

CC(=O)c1ccccc1O
2′-hydroxyacetophenone
CCOC(=O)c1c(C)c(C)cc(C=O)c1OC
3-ethyloxycarbonyldimethylmethyloxybenzaldehyde
CCOC(=O)c1c(C)c(C)cc(C=O)c1OC
material 7
CCOC(=O)c1c(C)c(C)cc(C=O)c1OC
3-ethyloxycarbonyldimethylmethyloxybenzaldehyde
→
COc1c(C=CC(=O)c2ccccc2O)cc(C)c(C)c1C(=O)O
1-[2-hydroxyphenyl]-3-[3-carboxydimethylmethyloxyphenyl]prop-2-en-1-one

Edukte

CC(=O)c1ccccc1O
2′-hydroxyacetophenone
CCOC(=O)c1c(C)c(C)cc(C=O)c1OC
3-ethyloxycarbonyldimethylmethyloxybenzaldehyde
CCOC(=O)c1c(C)c(C)cc(C=O)c1OC
material 7
CCOC(=O)c1c(C)c(C)cc(C=O)c1OC
3-ethyloxycarbonyldimethylmethyloxybenzaldehyde

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

This compound was synthesized from 2′-hydroxyacetophenone and 3-ethyloxycarbonyldimethylmethyloxybenzaldehyde (starting material 7) according to general method 2 described earlier.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07566737B2uspto-grants-2009_07