Reaktion #311719

Reaktionsgleichung

hydrogen sulphide

dodecene-1

→

n-dodecyl mercaptan

Lösungsmittel

diglyme

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigewere irradiated at 11° C
2. 2
   SonstigeAfter 3 minutes of irradiation

Vorschrift

Under the conditions of Example 3, with an input of 38 liters per hour of hydrogen sulphide, 67.7 mmoles of dodecene-1 dissolved in diglyme at a concentration of 0.564 mole per liter were irradiated at 11° C. After 3 minutes of irradiation, 48.2 mmoles of n-dodecyl mercaptan were formed.

Quelle