Reaktion #3062

Reaktionsgleichung

iminodiacetic acid dimethylester hydrochloride salt

N,N-diisopropyl-ethylamine

1,3-dibromopropane

→

title compound

Dimethyl N-(3-Bromopropyl)iminodiacetate

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigechromatographed

Vorschrift

A mixture of 1 mmol iminodiacetic acid dimethylester hydrochloride salt, 5 mmol N,N-diisopropyl-ethylamine and 3 mmol 1,3-dibromopropane in 2 mL toluene was stirred at 90° C. for 16 h and then chromatographed to provide the title compound as an oil.

Quelle