Reaktion #2765

Reaktionsgleichung

thiourea

neopentane

→

Thiourea neopentane

Lösungsmittel

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe solution with h/g crystals was removed from the autoclave
2. 2
   Filtrationfiltered
3. 3
   Waschenthe h/g crystals were washed with 10 ml cold ethanol
4. 4
   SonstigeThe h/g complex crystals were dried in the vacuum cabinet at 60° C.

Vorschrift

4 g thiourea were dissolved in 20 ml ethanol at 60° C. The solution was then placed in a high pressure autoclave and subjected to a neopentane pressure of 150 bar. The solution was cooled down to room temperature within 60 h. The solution with h/g crystals was removed from the autoclave, filtered and the h/g crystals were washed with 10 ml cold ethanol. The h/g complex crystals were dried in the vacuum cabinet at 60° C.

Quelle