Reaktion #2750

Reaktionsgleichung

4-propyl-4-phenyl-4-silacyclohexanone

4-chloro-2,6-difluorophenyltrimethylsilane

4-bromo-2,6-difluoro-1-(1,2-difluorovinyl)benzene

→

4'-(trans-4-n-propyl-4-silacyclohexyl)-2',6',3,5-tetrafluoro-4-(1,2-difluorovinyl)biphenyl

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigeobtaining the intended compound

Vorschrift

The general procedure of Example 35 was repeated using 4-propyl-4-phenyl-4-silacyclohexanone instead of 4-pentyl-4-phenyl-4-silacyclohexanone, 4-chloro-2,6-difluorophenyltrimethylsilane instead of 4-chlorophenyltrimethylsilane, and 4-bromo-2,6-difluoro-1-(1,2-difluorovinyl)benzene instead of 4-bromo-2,6-difluoro-1-(2,2-difluorovinyloxy)benzene, thereby obtaining the intended compound.

Quelle