Reaktion #2728

Reaktionsgleichung

1,2-dicyano-4-nitrobenzene

sodium phenoxide

→

1,2-Dicyano-4-phenoxybenzene

Ausbeute 49.0%

Lösungsmittel

dimethylformamide

Reaktionsbedingungen

Vorschrift

The procedure of Example 35 was followed except that 1,2-dicyano-4-nitrobenzene (1.0 part) was used in place of the 1,2-dicyano-3-nitrobenzene, 1.0 parts instead of 2.79 parts of sodium phenoxide and 20 parts instead of 50 parts of dimethylformamide were used. 1,2-Dicyano-4-phenoxybenzene (0.6 parts, 49%) was obtained as a white solid, m.pt.98°-100° C.

Quelle