Reaktion #2540

ord-faf03e3b2ef74ea6adbc16e6e6d66bc2

Reaktionsgleichung

Cc1cc(C)cc(N)c1
3,5-xylidine
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
Cc1cc(C)cc(NC(=O)c2ccc([N+](=O)[O-])cc2)c1
title compound
Cc1cc(C)cc(NC(=O)c2ccc([N+](=O)[O-])cc2)c1
4-Nitro-N-(3,5-dimethylphenyl)benzamide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using 3,5-xylidine (1.42 ml, 11.0 mmol) and 4-nitrobenzoic acid (1.76 g, 10.4 mmol), the procedure of Reference Example 16 was repeated to obtain 2.72 g (quantitative) of the title compound in the form of light yellow crystals.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03